Preparative binary pump HPLC system with UV and refractive index detector capabilities

NIH RePORTER · NIH · R15 · $77,283 · view on reporter.nih.gov ↗

Abstract

Our NIH-funded project (1 R15GM152969-01) focuses on synthesizing and characterizing fluorescent probes operating in the red to near-infrared region to measure pH levels within organelles. The current synthesis involves multiple steps, with silica gel chromatography causing delays and inefficiencies. The proposal suggests acquiring a preparative high-pressure liquid chromatography (HPLC) system to improve purification at each step, addressing the limitations of traditional silica gel column chromatography. The decision is driven by the complexity of the probes and the need for enhanced resolution in separating closely related compounds. The shift to preparative HPLC is expected to streamline the synthesis process and improve the overall efficiency of the project.

Key facts

NIH application ID
11034415
Project number
3R15GM152969-01S1
Recipient
MICHIGAN TECHNOLOGICAL UNIVERSITY
Principal Investigator
Rudy Lin Luck
Activity code
R15
Funding institute
NIH
Fiscal year
2024
Award amount
$77,283
Award type
3
Project period
2023-09-18 → 2026-08-31