Equipment Supplement: Methods and Strategies for the Concise Synthesis of Complex Alkaloid Natural Products

NIH RePORTER · NIH · R01 · $55,777 · view on reporter.nih.gov ↗

Abstract

Summary of the Request. We are requesting funds for the purchase of an Agilent 1260 Infinity II LC System to support our ongoing NIH project R01GM144663-03, “New Methods and Strategies for the Concise Synthesis of Complex Indole Alkaloids.” This advanced HPLC system, capable of solvent flow rates between 1-10 mL/min, is essential for both our primary analytical needs and semi-preparative applications. A reliable HPLC is critical for quantifying product ratios from various reactions, including diastereomers and distinct products, as well as determining enantiomeric ratios using chiral columns. Our current HPLC, an Agilent 1100 system purchased in 2005, has become increasingly unreliable, experiencing frequent leaks and severe pressure spikes that disrupt our research. The acquisition of the Agilent 1260 Infinity II LC System will ensure the accuracy and reliability of our analytical processes, thereby enhancing the quality and efficiency of our research. We respectfully request this supplement to maintain the high standards of our ongoing work and achieve the objectives outlined in our funded project.

Key facts

NIH application ID
11100962
Project number
3R01GM144663-04S1
Recipient
UNIVERSITY OF CHICAGO
Principal Investigator
VIRESH H. RAWAL
Activity code
R01
Funding institute
NIH
Fiscal year
2024
Award amount
$55,777
Award type
3
Project period
2021-09-10 → 2025-08-31