Exploiting Masked Alcohols to Guide Atom-Transfer Reactions

NIH RePORTER · NIH · R35 · $385,304 · view on reporter.nih.gov ↗

Abstract

ABSTRACT Fluorine incorporation into medicines, modern materials, and agricultural agents has improved their structural stability and reinvented these domains. Yet the world has not fully realized fluorine's potential. One promising approach to fluorine installation involves the direct transformation of a carbon–hydrogen bond (C–H bond) into a carbon–fluorine bond in a process known as C–H functionalization. Yet C–H functionalization processes have broader potential: they include reactions to replace C–H bonds with carbon–oxygen, carbon–sulfur, carbon–chlorine or carbon–carbon bonds. In short, C–H functionalization reactions are powerful technologies to streamline access to health-relevant small molecules. Over the last decade, some of the most important advances in C–H functionalization originated from new platforms to control the site of this reaction. Still, the utility of known C–H functionalization processes remains constrained by incomplete positional control in C–H functionalization processes. In some cases, positional control can be achieved by using a directing group. The proposed research includes new directing group strategies with the capacity to substantively extend the synthetic utility C–H functionalization reactions, with tremendous potential benefit to human health.

Key facts

NIH application ID
9955337
Project number
5R35GM128741-03
Recipient
DUKE UNIVERSITY
Principal Investigator
Jennifer L Roizen
Activity code
R35
Funding institute
NIH
Fiscal year
2020
Award amount
$385,304
Award type
5
Project period
2018-07-01 → 2023-06-30